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Picture of (+/-)-exo-6-Hydroxytropinone

(+/-)-exo-6-Hydroxytropinone

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Origin: China

Cas No: 5932-53-6

Specification: 99%min

Min order Quantity: 1 /kg

Supply Ability: 80 mt/month

Lead time: 7 days for OEM, 3 days for ready goods

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  • Products Specification
  • Product Description
  • Quick Details

    CAS No.:
    5932-53-6
    Other Names:
    6-HYDROXYTROPINONE
    MF:
    C8H13NO2
    EINECS No.:
    227-677-7
    Place of Origin:
    Shaanxi, China
    Type:
    Agrochemical Intermediates, Dyestuff Intermediates, Flavor & Fragrance Intermediates, Pharmaceutical Intermediates, Syntheses Material Intermediates
    Purity:
    99%min
    Brand Name:
    DIDAC
    Model Number:
    DAC170112
    Application:
    Pharm/Chem Industries
    Appearance:
    Liquid Form
    Structure Identification:
    H-NMR&LC-MS
    Identification:
    Infrared Absorption
    Test method:
    HPLC-ESI-MS
    Content:
    99.0% to 101.0%
    Water:
    0.5% Max.
    Sulfated ash:
    0.1% Max.
    Heavy metals:
    10ppm Max
    Total Impurity:
    0.2% Max.
    Assay:
    HPLC
    Disregard limit:
    0.0005%

    Packaging&Delivery

    Packaging Details
    25kgs/Drum; 200kgs/Drum
    Port
    Any main port of China

    Products Description

    Item
    Standard
    Test Results





    Identification
    A.H-NMR:Comply with the structure
    Complies
    B.LC-MS:Comply with the structure
    Complies
    C.The IR spectrum of sample should be identical with that of reference standard;
    Complies
    D.HPLC-ESI-MS
    The retention time of the major peak in the chromatogram of the Assay preparation corresponds to that in the chromatogram of the
    Standard preparation, as obtained in the Assay.
    Complies
    Crystallinity
    meets the requirements.
    Complies
    Loss on drying
    ≤2.0%
    0.19%
    Heavy metals
    ≤10 ppm
    <10ppm
    Water
    ≤1.0%
    0.1%
    Sulphated ash
    ≤0.5%, determined on 1.0 g.
    0.009%

    Related substances
    Unspecified impurities: for each impurity ≤0.10%
    <0.10%
    Total Impurity ≤0.5%
    0.18%
    Purity
    ≥99.0%
    99.7%
    Assay
    99.0%~101.0% (anhydrous substance).
    99.8%
    Storage
    Preserve in well-closed, light-resistant and airtight containers.
    Complies
  • Property

    CAS No.: 5932-53-6 Formula: C8H13NO2 Molecular Weight: 155.19400

    Basic Info

    Chemical Name (+/-)-exo-6-Hydroxytropinone
    Synonyms

    EXO-6-HYDROXYTROPINONE;
    6B-HYDROXY-3-TROPINONE;
    HYDROXYTROPINONE,6;
    Hydroxytropinone;
    6-HYDROXYTROPINONE;

    CAS No. 5932-53-6
    Molecular Formula C8H13NO2
    Molecular Weight 155.19400
    PSA 40.54000
    LogP -0.27920

    Properties

    Appearance & Physical State White powder.
    Density 1.217 g/cm3
    Boiling Point 291.6ºC at 760 mmHg
    Melting Point 120-123ºC
    Flash Point 130.1ºC
    Stability Stable under normal temperatures and pressures.
    Storage Condition Store in a tightly closed container. Store in a cool, dry, well-ventilated area away from incompatible substances.

    Safety Info

    Safety Statements S24/25
    WGK Germany 3
    Risk Statements R23/25

    Synthesis Route

    2,5-dimethoxy-2,5-dihydrofuran+1,3-Acetonedicarboxylic acid(+/-)-exo-6-Hydroxytropinone

    Precursor

    1,3-Acetonedicarboxylic acid
    2,5-dimethoxy-2,5-dihydrofuran
    methylamine hydrochloride

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