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D-(-)-3-thienylglycine

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Origin: China

Cas No: 1194-86-1

Specification: 99%min

Min order Quantity: 1 /kg

Supply Ability: 50 mt/month

Lead time: 7 days for OEM, 3 days for ready goods

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CAS No.: 1194-86-1 Formula: C6H7NO2S Molecular Weight: 157.19000

Description

D-(-)-3-Thienylglycine is used to prepare amide containing heterobicyclic metalloprotease inhibitors.

Basic Info

Chemical Name	D-(-)-3-thienylglycine
Synonyms	PIPECOLIC ACID; (R)-3-Thienylglycine; acidepipecolique; H-DL-HOPRO-OH; DL-HOMOPROLINE; DL-PIPECOLATE; H-DL-PIC(2)-OH; pipecolate; H-DL-HOMOPRO-OH; dihydrobaikiane;
CAS No.	1194-86-1
Molecular Formula	C6H7NO2S
Molecular Weight	157.19000
PSA	91.56000
LogP	1.53280

Properties

Density	1.435g/cm3
Boiling Point	383.8ºC at 760 mmHg
Flash Point	185.9ºC
Refractive Index	1.66
Vapor Pressure	1.41E-06mmHg at 25°C

Synthesis Route

(2S)-(-)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-2-(3-thienyl)essigsaeure→D-(-)-3-thienylglycine
3-formylthiophene→D-(-)-3-thienylglycine
(4S,5S)-(+)-2,2-Dimethyl-4-phenyl-5-<(3-thienylmethylen)amino>-1,3-dioxan→D-(-)-3-thienylglycine

Precursor

(2S)-(-)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-2-(3-thienyl)essigsaeure
(2S)-(+)-2-((4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino)-2-(3-thienyl)acetonitril
(4S,5S)-(+)-2,2-Dimethyl-4-phenyl-5-<(3-thienylmethylen)amino>-1,3-dioxan
3-formylthiophene

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