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Home > Organosulfur Compounds> 7-thiabicyclo[4.1.0]heptane
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7-thiabicyclo[4.1.0]heptane

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Origin: China

Cas No: 286-28-2

Specification: 99%min

Min order Quantity: 1 /kg

Supply Ability: 80 mt/month

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  • Products Specification
  • Product Description

  • Property

    CAS No.: 286-28-2 Formula: C6H10S Molecular Weight: 114.20900

    Basic Info

    Chemical Name 7-thiabicyclo[4.1.0]heptane
    Synonyms

    Cyclohexane,2-epithio;
    7-Thiabicyclo[4.1.0]heptane;
    Cyclohexene sulfide;
    1,2-epithiocyclohexane;
    cyclohexane sulfide;
    Cyclohexene episulfide;
    Cyclohexane,1,2-epithio;
    1,2-Cyclohexylene sulfide;

    CAS No. 286-28-2
    Molecular Formula C6H10S
    Molecular Weight 114.20900
    PSA 25.30000
    LogP 2.04440

    Properties

    Appearance & Physical State opalescent yellow liquid
    Density 1.09g/cm3
    Boiling Point 165.8ºC at 760mmHg
    Flash Point 50ºC
    Refractive Index n20/D 1.527(lit.)
    Storage Condition 0-6ºC
    Vapor Pressure 2.42mmHg at 25°C

    Safety Info

    Hazard Class 3.2
    Safety Statements S16
    HS Code 2934999090
    Packing Group III
    WGK Germany 3
    RIDADR UN 1993 3/PG 3
    Risk Statements R10

    Synthesis Route

    1,3-dimethylimidazolidine-2-thione+7-oxabicyclo[4.1.0]heptane→7-thiabicyclo[4.1.0]heptane+1,3-Dimethyl-2-imidazolidinone
    7-oxabicyclo[4.1.0]heptane→7-thiabicyclo[4.1.0]heptane
    trans-1-iodo-2-thiocyanatocyclohexane→7-thiabicyclo[4.1.0]heptane

    GC Analysis

    Column type Active phase Temperature (°C) Retention Index (I) Temperature Control Method
    Capillary Supelcowax-10 - 1390. temperature ramp

    Precursor

    ammonium thiocyanate
    cyclohexene
    1,3-dimethylimidazolidine-2-thione
    trans-1-iodo-2-thiocyanatocyclohexane

    Downstream Product

    (2R)-2-methoxy-2-phenylethanol
    Disulfide, bis(2-ethoxycyclohexyl)

    racem.-bis-(trans-2-hydroxy-cyclohexyl)-disulfide

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