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Picture of 3-Methoxybenzyl Chloride

3-Methoxybenzyl Chloride

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Origin: China

Cas No: 824-98-6

Specification: 99%min

Min order Quantity: 1 /kg

Supply Ability: 100 mt/month

Lead time: 7 days for OEM, 3 days for ready goods

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  • Products Specification
  • Product Description
  • Quick Details

    CAS No.:
    824-98-6
    Other Names:
    a-Chloro-m-methoxytoluene
    MF:
    C8H9ClO
    EINECS No.:
    212-541-1
    Place of Origin:
    Shaanxi, China
    Type:
    Agrochemical Intermediates, Dyestuff Intermediates, Flavor & Fragrance Intermediates, Pharmaceutical Intermediates, Syntheses Material Intermediates
    Purity:
    99%min
    Brand Name:
    DIDAC
    Model Number:
    DAC170112
    Application:
    Pharm/Chem Industries
    Appearance:
    Liquid Form
    Structure Identification:
    H-NMR&LC-MS
    Identification:
    Infrared Absorption
    Test method:
    HPLC-ESI-MS
    Content:
    99.0% to 101.0%
    Water:
    0.5% Max.
    Sulfated ash:
    0.1% Max.
    Heavy metals:
    10ppm Max
    Total Impurity:
    0.2% Max.
    Assay:
    HPLC
    Disregard limit:
    0.0005%

    Packaging&Delivery

    Packaging Details
    25kgs/Drum; 200kgs/Drum
    Port
    Any main port of China

    Products Description

    Item
    Standard
    Test Results





    Identification
    A.H-NMR:Comply with the structure
    Complies
    B.LC-MS:Comply with the structure
    Complies
    C.The IR spectrum of sample should be identical with that of reference standard;
    Complies
    D.HPLC-ESI-MS
    The retention time of the major peak in the chromatogram of the Assay preparation corresponds to that in the chromatogram of the
    Standard preparation, as obtained in the Assay.
    Complies
    Crystallinity
    meets the requirements.
    Complies
    Loss on drying
    ≤2.0%
    0.19%
    Heavy metals
    ≤10 ppm
    <10ppm
    Water
    ≤1.0%
    0.1%
    Sulphated ash
    ≤0.5%, determined on 1.0 g.
    0.009%

    Related substances
    Unspecified impurities: for each impurity ≤0.10%
    <0.10%
    Total Impurity ≤0.5%
    0.18%
    Purity
    ≥99.0%
    99.7%
    Assay
    99.0%~101.0% (anhydrous substance).
    99.8%
    Storage
    Preserve in well-closed, light-resistant and airtight containers.
    Complies
  • Property

    CAS No.: 824-98-6 Formula: C8H9ClO Molecular Weight: 156.60900

    Description

    3-Methoxybenzyl chloride is a chemical reagent used to benzylate sugars (e.g. 2-Deoxy-D-ribose [D252000]) and also used to alkylate amides (e.g. Benzyl acetoacetic amide [B222950]).

    Basic Info

    Chemical Name 3-Methoxybenzyl Chloride
    Synonyms

    1-(chloromethyl)-3-methoxybenzene;

    CAS No. 824-98-6
    Molecular Formula C8H9ClO
    Molecular Weight 156.60900
    PSA 9.23000
    LogP 2.43400

    Properties

    Appearance & Physical State clear colorless to light yellow liquid
    Density 1.078
    Boiling Point 124ºC (13 mmHg)
    Melting Point 101.67ºC
    Flash Point 101ºC
    Refractive Index 1.543-1.545
    Stability Stable under normal temperatures and pressures.
    Storage Condition Store at 0-5ºC

    Safety Info

    Hazard Class 8
    Safety Statements S26-S36/37/39-S45
    HS Code 29093090
    WGK Germany 1
    Packing Group III
    RIDADR UN 3265
    Risk Statements R34
    Hazard Codes C

    Synthesis Route

    4-Formylmorpholine+BENZENEMETHANOL, 3-METHOXY-, 1-METHANSULFONATE3-Methoxybenzyl Chloride
    3-Methoxybenzyl Alcohol3-Methoxybenzyl Chloride
    1-methoxy-3-(methoxymethyl)benzeneMethyl acetate+3-Methoxybenzyl Chloride

    Precursor

    BENZENEMETHANOL, 3-METHOXY-, 1-METHANSULFONATE
    1-methoxy-3-(methoxymethyl)benzene
    1-(dimethoxymethyl)-3-methoxybenzene
    3-Methoxybenzyl Alcohol

    Downstream Product

    1-(3-Methoxybenzyl)piperazine
    1-[(3-methoxyphenyl)methyl]pyridin-1-ium,chloride
    Diethyl (3-Methoxybenzyl)phosphonate
    1-methoxy-3-(3-methylbut-3-enyl)benzene

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