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Di-tert-Butyl azodicarboxylate

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Origin: China

Cas No: 870-50-8

Specification: 99%min

Min order Quantity: 1 /kg

Supply Ability: 100 mt/month

Lead time: 7 days for OEM, 3 days for ready goods

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  • Products Specification
  • Product Description

  • Property

    CAS No.: 870-50-8 Formula: C10H18N2O4 Molecular Weight: 230.26100

    Description

    Di-tert-butyl azodicarboxylate is a reagent used in the preparation of acyl hydrazinedicarboxylates via photoorganocatalytic hydroacylation of dialkyl azodicarboxylates with aldehydes in presence of phenylglyoxylic acid as photocatalyst.

    Basic Info

    Chemical Name Di-tert-Butyl azodicarboxylate
    Synonyms

    di-tert-butylazadicarboxylate;
    di-tert-butylazodicarboxylate;
    DI-TERT-BUTYL AZODICARBOXYALTE;
    DI-T-BUTYL AZODICARBOXYLATE;
    tBuO2CN=NCO2tBu;
    Boc-N=N-Boc;
    Di-tert-Butyl azodic;
    tert-butyl azodicarboxylate;

    CAS No. 870-50-8
    Molecular Formula C10H18N2O4
    Molecular Weight 230.26100
    PSA 77.32000
    LogP 3.30880

    Properties

    Appearance & Physical State yellow crystals or crystalline powder
    Density 1.06 g/cm3
    Boiling Point 287.1ºC at 760 mmHg
    Melting Point 90-92ºC
    Flash Point 107.2ºC
    Refractive Index 1.459
    Water Solubility Insoluble
    Storage Condition 2-8ºC

    Safety Info

    Safety Statements S16-S26-S37/39
    HS Code 2927000090
    WGK Germany 3
    RIDADR UN 1325
    Risk Statements R11; R36/37/38
    Hazard Codes F; Xi
    Caution Statement P261; P305 + P351 + P338
    Signal Word Warning
    Symbol GHS07
    Hazard Declaration H315; H319; H335

    Synthesis Route

    DI-Tert-Butyl Hydrazodicarboxylate→Di-tert-Butyl azodicarboxylate
    tert-butoxycarbonyl anhydride→Di-tert-Butyl azodicarboxylate
    DI-Tert-Butyl Hydrazodicarboxylate+bis(acetato-O)triphenylbismuth(V)→Di-tert-Butyl azodicarboxylate

    Precursor

    DI-Tert-Butyl Hydrazodicarboxylate
    bis(acetato-O)triphenylbismuth(V)
    tert-butoxycarbonyl anhydride

    Downstream Product

    DI-Tert-Butyl Hydrazodicarboxylate
    ditert-butyl 3,6-dihydropyridazine-1,2-dicarboxylate
    ditert-butyl 2,3-diazabicyclo[2.2.1]heptane-2,3-dicarboxylate
    1-pyridin-2-ylpiperazin-2-one

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