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cuscohygrine

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Origin: China

Cas No: 454-14-8

Specification: 99%min

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  • Products Specification
  • Product Description
  • Property

    CAS No.: 454-14-8 Formula: C13H24N2O Molecular Weight: 224.34200

    Description

    Cuscohygrine is a pyrrolidine alkaloid found in coca. It can also be extracted from plants of the family Solanaceae as well, including Atropa belladonna (deadly nightshade), Datura inoxia and Datura stramonium (jimson weed). Cuscohygrine usually occurs along with other, more potent alkaloids such as atropine or cocaine.
    Cuscohygrine, along with the related metabolite hygrine, was first isolated by Carl Liebermann in 1889 as an alkaloid accompanying cocaine in coca leaves (also known as Cusco-leaves).
    Cuscohygrine is an oil that can be distilled without decomposition only in vacuum. It is soluble in water. It also forms a crystalline trihydrate which melts at 40–41°C.

    Basic Info

    Chemical Name cuscohygrine
    Synonyms

    2-Propanone, 1,3-bis(1-methyl-2-pyrrolidinyl)-, (R*,S*)-;
    Hellaradine;
    Cuscohygrine;
    Cuskhygrine;

    CAS No. 454-14-8
    Molecular Formula C13H24N2O
    Molecular Weight 224.34200
    PSA 23.55000
    LogP 1.39990

    Properties

    Density 0.989 g/cm3
    Boiling Point 312.4ºC at 760 mmHg
    Refractive Index 1.488
    Stability Solutions are unstable.
    Storage Condition -20ºC Freezer
    Vapor Pressure 0.000531mmHg at 25°C

    Safety Info

    HS Code 2933990090

    Synthesis Route

    1,3-bis-(1-methyl-pyrrol-2-yl)-acetonecuscohygrine
    N-methylpyrrolidin-2-one+1,3-Acetonedicarboxylic acidcuscohygrine
    1,3-Acetonedicarboxylic acid+4-methylamino-butyraldehydecuscohygrine

    GC Analysis

    Column type Active phase Temperature (°C) Retention Index (I) Temperature Control Method
    Capillary DB-1 - 1650. temperature ramp
    Capillary OV-1 - 1650. temperature ramp
    Capillary DB-1 - 1650. temperature ramp
    Capillary OV-1 - 1650. custom temperature program

    Precursor

    4-methylamino-butyraldehyde
    N-methylpyrrolidin-2-one
    1,3-Acetonedicarboxylic acid
    1,3-bis-(1-methyl-pyrrol-2-yl)-acetone

    Downstream Product

    undecane
    6-UNDECANOL
    N-(4-methoxy-6-oxo-1H-2,1,3-benzoxadiazol-7-yl)acetamide

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