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[5-chloro-2-(cyclopropylmethylamino)phenyl]-phenylmethanone

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Origin: China

Cas No: 2897-00-9

Specification: 99%min

Min order Quantity: 1 /kg

Supply Ability: 80 mt/month

Lead time: 7 days for OEM, 3 days for ready goods

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Product Description

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CAS No.: 2897-00-9 Formula: C17H16ClNO Molecular Weight: 285.76800

Description

2-Cyclopropylmethylamino-5-chlorobenzophenone is a benzodiazepine derivative.

Basic Info

Chemical Name	[5-chloro-2-(cyclopropylmethylamino)phenyl]-phenylmethanone
Synonyms	2-N-cyclopropmethylamino-5-chloro-benzophenone; 2-Cyclopropylmethylamino-5-chlorbenzophenon; 5-chloro-2-cyclopropylmethylaminobenzophenone; 2-CYCLOPROPYLMETHYLAMINO-5-CHLOROBENZOPHENONE;
CAS No.	2897-00-9
Molecular Formula	C17H16ClNO
Molecular Weight	285.76800
PSA	29.10000
LogP	4.46590

Properties

Density	1.252
Boiling Point	469.6ºC at 760 mmHg
Melting Point	79-80ºC
Refractive Index	1.641
Vapor Pressure	5.42E-09mmHg at 25°C

Safety Info

HS Code	2922399090

Synthesis Route

7-chloro-1-(cyclopropylmethyl)-3-hydroxy-5-phenyl-3H-1,4-benzodiazepin-2-one→2-Amino-5-chlorobenzophenone+[5-chloro-2-(cyclopropylmethylamino)phenyl]-phenylmethanone
7-chloro-1-(cyclopropylmethyl)-5-phenyl-3H-1,4-benzodiazepin-2-one→2-Amino-5-chlorobenzophenone+[5-chloro-2-(cyclopropylmethylamino)phenyl]-phenylmethanone
5-chloro-2-cyclopropylmethylaminobenzophenone imine+Trichloroacetyl Chloride→6-chloro-1-cyclopropylmethyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone+6-chloro-1-(cyclopropylmethyl)-4-phenylquinazolin-2-one

GC Analysis

Column type	Active phase	Temperature (°C)	Retention Index (I)	Temperature Control Method
Capillary	BP-1	200.	2349.	isothermal
Packed	SE-30	220.	2370.	isothermal
Packed	SE-30	250.	2398.	isothermal
Capillary	Cross-Linked Methylsilicone	-	2410.	temperature ramp
Capillary	HP-5MS	-	2410.	custom temperature program

Precursor

7-chloro-1-(cyclopropylmethyl)-3-hydroxy-5-phenyl-3H-1,4-benzodiazepin-2-one
Trichloroacetyl Chloride
5-chloro-2-cyclopropylmethylaminobenzophenone imine
carbon monoxide

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