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4-TBSMS-hydroxymethylphenylboronic acid

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Origin: China

Cas No: 162356-89-0

Specification: 99%min

Min order Quantity: 1 /kg

Supply Ability: 100 mt/month

Lead time: 7 days for OEM, 3 days for ready goods

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CAS No.: 162356-89-0 Formula: C13H23BO3Si Molecular Weight: 266.21600

Basic Info

Chemical Name	4-TBSMS-hydroxymethylphenylboronic acid
Synonyms	[4-[[tert-butyl(dimethyl)silyl]oxymethyl]phenyl]boronic acid;
CAS No.	162356-89-0
Molecular Formula	C13H23BO3Si
Molecular Weight	266.21600
PSA	49.69000
LogP	1.88820

Properties

Melting Point	153-155ºC
Refractive Index	1.509

Safety Info

HS Code	2931900090

Synthesis Route

8-(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)-4-methyl-2,6-dioxohexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide→4-TBSMS-hydroxymethylphenylboronic acid
(4-bromophenyl)methoxy-tert-butyl-dimethylsilane→4-TBSMS-hydroxymethylphenylboronic acid
4-Bromobenzyl alcohol→4-TBSMS-hydroxymethylphenylboronic acid

Precursor

tert-butyldimethylsilyl chloride
4-Bromobenzyl alcohol
8-(4-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)-4-methyl-2,6-dioxohexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide
(4-bromophenyl)methoxy-tert-butyl-dimethylsilane

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