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(+)-AROMADENDRENE

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Origin: China

Cas No: 489-39-4

Specification: 99%min

Min order Quantity: 1 /kg

Supply Ability: 80 mt/month

Lead time: 7 days for OEM, 3 days for ready goods

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CAS No.: 489-39-4 Formula: C15H24 Molecular Weight: 204.35100

Basic Info

Chemical Name	(+)-AROMADENDRENE
Synonyms	alloaromadendrene; aromadenderene; aromandendrene;
CAS No.	489-39-4
Molecular Formula	C15H24
Molecular Weight	204.35100
PSA	0.00000
LogP	4.27090

Properties

Density	0.93g/cm3
Boiling Point	261-263ºC(lit.)
Melting Point	262ºC
Flash Point	106.5ºC
Refractive Index	n20/D 1.497
Storage Condition	2-8ºC

Safety Info

WGK Germany	3

Synthesis Route

((1aR,4S,4aR,7R,7aR,7bS)-1,1,7-trimethyldecahydro-1H-cyclopropa[e]azulen-4-yl)methyl methanesulfonate→(+)-AROMADENDRENE
methyl (+)-(1S,7R)-8,8-dimethyl-3-oxobicyclo<5.1.0>octane-4-carboxylate→(+)-AROMADENDRENE
(+)-(1S,2S,4R,7R)-4-tert-butyldimethylsiloxymethyl-8,8-dimethyl-2-(2-propenyl)bicyclo<5.1.0>octan-3-one→(+)-AROMADENDRENE

GC Analysis

Column type	Active phase	Temperature (°C)	Retention Index (I)	Temperature Control Method
Capillary	DB-1	150.	1455.	isothermal
Capillary	DB-Wax	-	1635.	temperature ramp
Capillary	HP-5MS	-	1440.	temperature ramp
Capillary	DB-1	-	1439.	temperature ramp
Capillary	HP-5	-	1441.	temperature ramp

Precursor

(+)-(1R,2R,4R,7S)-7-tert-butyldimethylsiloxymethyl-3,3-dimethyltricyclo(6.3.0.02,4)undec-8-en-10-one
(+)-(1S,2S,4R,7R)-4-tert-butyldimethylsiloxymethyl-8,8-dimethyl-2-(2-oxopropyl)bicyclo[5.1.0]octan-3-one
(+)-(1S,2S,4R,7R)-4-tert-butyldimethylsiloxymethyl-8,8-dimethyl-2-(2-propenyl)bicyclo<5.1.0>octan-3-one
((1aR,4S,4aR,7R,7aR,7bS)-1,1,7-trimethyldecahydro-1H-cyclopropa[e]azulen-4-yl)methyl methanesulfonate

Downstream Product

(-)-GLOBULOL
isoledene
(+)-γ-GURJUNENE
(1aR,4aR,7S,7aR,7bR)-1,1,7-Trimethyl-4-methylenedecahydro-1H-cycl opropa[e]azulen-7-ol

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